Rapid Estimation of <i>T</i><sub>1</sub> for Quantitative NMR
نویسندگان
چکیده
Quantitative NMR spectroscopy (qNMR) is an essential tool in organic chemistry, with applications including reaction monitoring, mechanistic analysis, and purity determination. Establishing the correct acquisition rate for consecutive qNMR scans requires knowledge of longitudinal relaxation time constants (T1) all nuclei being monitored. We report a simple method that about 10-fold faster than conventional inversion recovery technique estimation T1.
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ژورنال
عنوان ژورنال: Journal of Organic Chemistry
سال: 2021
ISSN: ['1520-6904', '0022-3263']
DOI: https://doi.org/10.1021/acs.joc.1c01007